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By reaction of carbon tetrachloride with lithium tris(trimethylsilyl)hydrazide and then with lithium butyl a compound with formula (Me 3 Si) 2 N 2 C is formed. From the way of preparation, spectroscopic investigations, and chemical reactions the substance is characterized as bis(trimethylsilyl)aminoisocyanide (3). 3 hydrolyzes, and does not react with oxygen. The compound combines with chlorine and bromine forming aminoisocyanide dihalides, and with carbon disulfide forming an adduct. At higher temperatures 3 isomerizes to bis(trimethylsilyl)carbodiimide (1).

zeitschrift für naturforschung b

Über Derivate des Hydrazins, VI I  Darstellung und Charakterisierung von Bis(trimethylsilyl)aminoisocyanid.: On Derivatives of Hydrazide, VI 1  Preparation and Characterization of Bis(trimethylsilyl)aminoisocyanide