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Direct and sensitized photolysis of 2-(a- diazo-benzyl)-pyridine-1-oxide (2) as well as its thermolysis in deoxygenated solvents resulted 2-benzoylpyridine (3) in nearly quantitative yield. As a geometrical consequence of the intramolecular abstraction of oxygen from the N→O group by the triplet carbene (1) the formation of an oxazetine intermediate (4) is discussed.

Notizen: Photolyse und Thermolyse von 2-(α-Diazo-benzyl)-pyridin-1-oxid / Photolysis and Thermolysis of 2- (α-Diazo-benzyl) -pyridine-1-oxide