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FeNb 11 O 29 (m), FeNb 11 O 29 (o) and two mixed oxides with the composition limits FeNb 29 O 74  and TiNb 14 O 37  were prepared by chemical transport. The crystal structures of the compounds have been examined by two-dimensional high resolution electron-microscopy. They are composed of ‘blocks’ of (n × 3) corner shared octahedra and belong to a series of structure related compounds with the general formula Me 3n O 8n-3 . Crystallographic defects and the thermic behavior of the materials are discussed.

zeitschrift für naturforschung b

Beiträge zur Untersuchung anorganischer nichtstöchiometrischer Verbindungen, V. Präparative und elektronenoptische Untersuchungen an FeNb 11 O 29 , FeNb 29 O 74  und TiNb 14 O 37 .: Contributions to the Study of Inorganic Non-Stoichiometric Compounds, V. Preparation and Electron Optical Investigation of FeNb 11 O 29 , FeNb 29 O 74  and TiNb 14 O 37