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γ-Thiovalerolactone (1), under high pressure (15 kbar, 170°C), forms the compounds 2 and 3. Under similar conditions, δ-thiovalerolactone polymerizes nearly quantitatively; at 11 kbar and 170°C, 5 is formed in 2% yield. Thiooxindole 7 reacts to yield 8 and the thermically very stable trimer 9.

zeitschrift für naturforschung b

Notizen: Hochdruckreaktionen, ΧII / High Pressure Reactions, XII: Verhalten von Thiolactonen und ausgewählten schwefelhaltigen Heterocyclen unter hohen Drucken / Behaviour of Thiolactones and Selected Sulphur Containing Heterocycles at High Pressures