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Starting with ( 14 C)chloroform 1,2,3,3-tetrachloro-(1,3- 14 C)-1-propene (7 z) with unsymmetrical distribution of  14 C is synthesized according reaction scheme 1. 7 z is isomerized with AlCl 3  to 1,2,3,3-tetrachloro-(1,3- 14 C)-1-propene (7 t) with symmetrical distribution of  14 C. From 7 z and 7 t the dichloro-( 14 C)acetanilides (13 z) and (13 t) are formed via the dichloro-( 14 C) acetic acids. The distribution of  14 C on C-1 (75%) and C-3 (25%) from 7 z follows from comparison of the activities of 13 z, 13 t with 7 z.

zeitschrift für naturforschung b

Markierte Verbindungen, XXII 1  1.2.3.3-Tetrachlor-(1.3- 14 C)-1-propen mit unsymmetrischer  14 C-Verteilung / On Labelled Compounds, XXII l,2,3,3-Tetrachloro-(1,3- 14 C)-1-propene with Unsymmetrical Distribution of  14 C