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New adducts of nitrogen triiodide with several tertiary N-bases have been prepared. Their analyses, general properties, IR-spectra and structures are reported briefly. Experiments to crystallize a compound with a ratio N : I : chinuclidin = 1 : 4 : 1 resulted in the preparation of cristallized chinuclidiniumpentaiodide (chin H)I 3  • I 2 , the X-ray structure analysis of which is reported.

zeitschrift für naturforschung b

Untersuchungen an Stickstoff-Jod-Verbindungen, XV Neue Addukte des Stickstofftrijodids mit tertiären N-Basen-Chinuclidiniumpentajodid (Chin H)J 3  · J 2 , ein neues Polyjodid / Studies on Nitrogen-Iodine Compounds, XV New Adducts of Nitrogen Triiodide with Tertiary N-Bases-Chinuclidiniumpentaiodide (Chin H)I 3  · I 2 , a New Polyiodide