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Single crystals of Cu 4 V 2.15 O 9,38  were prepared by hydrothermal synthesis. The composition was confirmed by analysis and crystal structure investigation. Cu 4 V 2.15 O 9,38  has an orthorhombic unit cell : a = 15.021, b = 8.564 and c = 6.055 Å, space group D 2  4 P 2 1 2 1 2 1 . The structure consists of a network made up of chains of edge-shared Cu-O 6  octahedra. The chains are linked by Cu-O 6  octahedra building up a wave-like layer parallel to the b/c plane. The layers are linked to each other by V—O 4  tetrahedra and two sorts of trigonal bipyramids one of them containing copper. The center of the other one is statistically filled with vanadium.

Über ein neues Kupfervanadat: Cu 4 V 2.15 O 9.38 / About Cu 4 V 2,15 O 9.38