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Crystals of [Fe(NO) 2 PØ 3 Cl] are monoclinic with a = 1.6265(7) [nm], b = 1.4495(7) [nm], c = 1.5609(6) [nm] and β= 96.86(2) deg.; the space group is C 2/c. The structure was determined by three dimensional Patterson and Fourier methods on the basis of 2266 independent intensities. The unit cell consists of 8 isolated molecules. Within the coordination polyhedron, a distorted trigonal pyramid, the Cl, Fe, P plane approximately represents a mirror plane of the molecule. The nitrosyl ligands are bent towards each other with an N-Fe-N angle of 115.6(3) and Fe-N-O angles of 166.4(5) and 165.5(5) deg. The geometry of the molecule is discussed with regard to other dinitrosyl complexes and to electronic structure.

zeitschrift für naturforschung b

Kristall- und Molekülstruktur des Chlorodinitrosyltriphenylphosphineisens(-I) / Crystal and Molecular Structure of Chlorodinitrosyltriphenylphosphineiron(-I)