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Upon irradiation of C 5 H 5 V(CO) 4  in the presence of the Schiff base, derived from pyridine-carbaldehyde (2) and S-(—)-α-methylbenzyl-amine, two cis CO groups are replaced by the chelating ligand with the formation of complex 3. The reaction of C 5 H 5 W(CO) 3 Cl with 8-hydroxy-quinoline in boiling THF yields the oxinato complex 4. The analogous compound 5 is obtained in the reaction of C 5 H 5 Mo(CO) 3 Cl with 7-carboxy-8-hydroxyquinoline.

zeitschrift für naturforschung b

Optisch aktive Übergangsmetall-Komplexe, XXII: Asymmetrische Komplexe von Vanadin, Molybdän und Wolfram mit quadratisch-pyramidaler Struktur / Asymmetric Complexes of Vanadium, Molybdenum and Tungsten with Square Pyramidal Structure