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The photoelectron(PE) spectra of methylthio- (X = SCH 3 ) and methoxyboranes (X = OCH 3 ) (CH 3 ) 3-n BX n  are compared and assigned by means of modified CNDO/2 calculations. Substituent effects on π-orbitals and chemical shifts (δ 11 B) confirm the existence of non-negligible π-contributions to the boron-sulphur bond.

zeitschrift für naturforschung b

Photoelektronenspektroskopische Untersuchungen an Bor-Verbindungen, I / Photoelectronspectroscopic Investigations on Boron Compounds, I: Orbitalreihenfolgen und Ladungsdichten in Methylthio- und Methoxyboranen / Orbitalsequences and Charge Densities of Methylthioand Methoxyboranes