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Polymeric MoO 2  (O 2 PCl 2 ) · POCl 3  1 is obtained by the reaction of MoCl 5  and P 2 O 3 Cl 4 , while MoO 2 Cl 2  · POCl 3  2 is formed by passage of Cl 2 O into a solution of MoCl 5  in POCl 3 . From magnetic measurements and IR data it appears that 1 contains no Mo-O-Mo system but Mo-O-P-O-Mo bridges. The IR and RAMAN spectra of 2 were assigned by comparison with the spectrum of MoO 2 Cl 2  · H 2 O.

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Darstellung, Eigenschaften und Schwingungsspektren von MoVO 2 (O 2 PCl 2 ) · POCl 3  und MoO 2 Cl 2  · POCl 3  / Preparations, Chemical Properties and the Vibrational Spectra of MoVO 2 (O 2 PCl 2 ) · POCl 3  und MoO 2 Cl 2  · POCl 3