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Fe (PF 3 )  5  reacts with halogens to yield the dihalogeno-tetrakis (trifluorophosphine) -iron complexes X 2 Fe (PF 3 ) 4  (X = Cl, Br, J). The structure of the volatile cristalline compounds is octahedral with the halogen atoms in cis-position. The IR-, Mass- and F-NMR-spectra are reported and discussed; the Mössbauer-spectra are listed.

zeitschrift für naturforschung b

Metalltrifluorphosphin-Komplexe, XXXI / Metaltrifluorophosphine Complexes, XXXI: Halogenderivate von Pentakis(trifluorphosphin)-eisen(0) / Halogen Derivatives of Pentakis (trifluorophosphine)-Iron (0)