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The crystal structure of Di-µ-hydroxy-bis [aquo-triamminecobalt (III)] nitrate-2-hydrate has been determined by x-ray diffraction using counter techniques. The compound crystallizes in the monoclinic space group C 2h  5 -P2 1 /n with a=9.444 (2), b=9.684 (3), c=10.736 (3) Å, β=90.1 (2)°, Z= 2. A total of 1765 independent reflections was used in solving the structure, which was refined to a conventional R 1 -factor of 0.047. It was not possible to distinguish by x-ray methods between the oxygen and nitrogen atoms of the NH 3 - and H 2 O molecules in the complex cation, because of their similarity in point of electrostatical and spatial behaviour.

zeitschrift für naturforschung b

Die Kristallstruktur von Di-μ-hydroxo-bis[aquotriamminkobalt(III)]-nitrat-2-Hydrat / The Crystal Structure of Di-μ-hydroxo-bis[aquotriamminecobalt (III)] - nitrate-2-hydrate