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The polarographic reduction of C 5 H 5 NiNO in DMF and ACN has been investigated. The first step of reduction involves an irreversible transfer of one electron to form an instable radical anion. On the basis of polarographic, voltammetric and coulometric measurements an overall mechanism is suggested.

Polarographic Behaviour of Transition Metal Nitrosyl Complexes in Nonaqueous Media. IV. Cyclopentadienylnitrosylnickel