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The structure of radicals in X-irradiated polycrystalline phosphonic acid esters (trichlorphontype) and trichlorphon single crystals has been investigated by ESR. At room temperature in trichlorphon the radical (R0) 2  &gt; P(O) - CHOH - ĊCl 2  (R = CH 3 ) is formed by removal of a chlorine atom. The g-factor is 2,010 and the hyperfine parameters are α H  β = 7 ± 0,5 G for the isotropic β-proton and α CL = 7 - 14 G for the two anisotropic chlorine atoms.

zeitschrift für naturforschung b

Strahleninduzierte freie Radikale in phosphoroorganischen Verbindungen II: Struktur freier Radikale in Trichlorphon nach Röntgenbestrahlung bei Zimmertemperatur / Structure of Free Radicals in Trichlorphon X-Irradiated at Room Temperature