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The NMR solid-echo polycrystalline tris-guanidinium nonachlorodiantimonate (III) has been studied in a wide temperature range. The temperature dependences of a time position and an amplitude of solid-echo are characterized by minima at ca. 143 K and 273 K, which are assigned to the reorientation of two dynamically inequivalent guanidinium cations [C(NH 2 ) 3 ] + . The motional parameters of the two types of guanidinium cations have been determined. -PACS: 64.70K; 76.60.E

An NMR solid-echo Study of Guanidinium Cation Reorientation in [C(NH 2 ) 3 ] 3 Sb 2 Cl 9