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Inelastic incoherent neutron scattering (IINS) spectra and neutron powder diffraction (NPD) patterns, registered for [Co(H 2 O) 6 ](ClO 4 ) 2  at 18 -270 K and for [Mn(H 2 O) 6 ](BF 4 ) 2  at 18 -230 K, provided evidence that these crystals possess three solid phases in these ranges of temperatures. In both compounds the phase transition occurring at T C3  is connected with a change of the crystal structure, and that occurring at T C2  with a change in the rate of the reorientational motions of H 2 O ligands.

Phase Transitions and Water Dynamics of [Co(H 2 O) 6 ](ClO 4 ) 2 and [Mn(H 2 O) 6 ](BF 4 ) 2 Studied by Neutron Scattering Methods