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The temperature variations of the  63 Cu,  65 Cu and  51 V NMR spectra and  51 V spin-lattice relaxation rate 1/T 1  have been measured in a thiospinel CuV 2 S 4  . Drastic changes in the spectra and relaxation rates were observed at the charge density wave (CDW) transition temperature. With decreasing temperature T, 1/T 1  decreases exponentially due to the CDW transition (75 K &lt; T&lt; 90 K). The energy gap made by the CDW formation at 90 K is estimated to be 0.052 eV from an Arrhenius plot of 1/T 1 .

Change in 51 V Relaxation Rates due to CDW in CuV 2 S 4