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Nuclear magnetic resonance (NMR) of  51 V and  209 Bi, and electron paramagnetic resonance (EPR) of Mn 2+  and Fe 3+  impurities in ferroelastic BiVO 4  single crystals are reviewed. The nuclear quadrupole parameters and principal axes of the two host nuclei,  51 V and  209 Bi, and the second-or-der zero field splitting tensor of the isoelectronic 3 d 5  ions, Mn 2+  and Fe 3+  , in BiVO 4  are determined for the first time. Temperature dependence studies on  51 V NMR and Mn 2+  EPR confirmed that this crystal undergoes a second order phase transition. The substitutional sites of Mn 2+  and Fe 3+  in BiVO 4  are Bi 3+  and V 5+ , respectively.

Magnetic Resonances of 51 V, 209 Bi, Mn 2+ , and Fe 3+ in BiVO 4 Single Crystals