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The rotational spectrum of  33 S anti-2,3-dimethylthiirane with its  33 S nuclear quadrupole coupling hyperfine structure in the range 7.6 to to 21.5 GHz and its analysis is reported. The rotational constants are A = 5331.1401(5), B = 3506.3963(10), and C = 2356.9273(2) MHz. The  33 S quadrupole coupling constants are χ aa  = 8.3871(93), χ bb  = -32.3291(174), and χ cc  = 23.9420(174) MHz.

The 33 S Nuclear Quadrupole Coupling in the Rotational Spectrum of anti-2,3-Dimethylthiirane