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The electronic absorption spectra of the solid tetrabutylammonium salts of [OsCl n Br 6-n  ] 2- , n = 0-6, including the stereoisomers for n = 2, 3, 4, are measured at 10 K. The weak intraconfigurational excitations within the t 2g  4 , manifold of Os(lV) are split by spin orbit coupling and lowered symmetry into multiplets, observed in the NIR regions 2600-3100, 4800-5400, 10 500-11 400 and 16 000 17 200 cm -1 . The 0-0-transitions are deduced from vibrational fine structure and they are confirmed by electronic Raman bands with the same frequencies

Absorptions- and Electronic Raman Spectra of Chloro- Bromo-Osmate (IV), [OsCl n Br 6-n J 2- , n=0-6