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127 I solid state NMR studies revealed second order quadrupole effects in (C 2 H 5 ) 4 SbIO 4  with anomalous positive temperature coefficients of the quadrupole coupling constants. This anomaly is caused by a continuous change of the axes of the electric field gradient tensor.

Anomalous Temperature Dependence of the 127 I Quadrupole Interaction in Tetraethylstiboniummetaperiodate (C 2 H 5 ) 4 SbIO 4