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6  polarized β-active  8 Li probe nuclei were produced by capture  of polarized thermal neutrons. Nuclear magnetic resonance spectra of  8 Li were recorded via the  β-radiation asymmetry. The   8 Li quadrupole coupling constant e 2 qQ/h , measured in the  temperature range T = 5 . .. 500 K decreases with increasing 7 from 45.2(8) to 22.8(4) kHz.  Anomalies in the overall temperature dependence are discussed in terms of phase transitions  proposed for LiC 6 .

ß-NMR Study of the Electric Field Gradient in the Metallic Intercalation Compound LiC 6