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The title compound has been prepared by elemental synthesis at high temperatures and also by reaction of Na 4 P 2 S 6  · 6H 2 O with CsCl in aqueous solution. Both reaction products have closely related vibrational spectra which are assigned on the basis of a P 2 S 6  4-  anion with perturbed D 3d  symmetry. A normal coordinate analysis has been performed using a force Field with 4 initial force constants. The refined force Field, potential energy distribution (PED), mean amplitudes of vibration and Coriolis coupling constants are given.

Synthesis, Vibrational Spectra and Normal Coordinate Analysis of Cesium-Hexathiohypodiphosphate Cs 4 P 2 S 6