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The Zeeman effect of the nuclear quadrupole resonance (NQR) lower transition (± 3/2 ↔ 1/2) spectrum for I=5/2 in crystalline powder has been studied and the frequency splittings of the ±3/2 ↔ ± 1/2 transition line have been plotted as a function of the asymmetry parameter η and the external magnetic field H. The experimental Zeeman frequency splittings of the  127 I lower transition line in crystalline powder of H 5 IO 6  have been compared with the theoretical values in order to evaluate η. The present value of η agrees with the earlier values reported from the two transition frequencies and also from a single crystal Zeeman study on the ± 3/2 ↔ ± 1/2 transition line.

Powder Zeeman Study of the Nuclear Quadrupole Resonance Lower Transition Spectrum for I = 5/2; Application to Orthoperiodic Acid