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A crystal structure refinement for CsGaCl 4  resulted in considerably lower limits of error than older data from the literature. These were used for a superposition analysis of EPR data for Fe 3+  in this compound. The experimental zero field splitting (ZFS) pattern could be very satisfactorily reproduced with the intrinsic ZFS parameter b̅ 2  = 0.6 cm -1 . Thus like for other ligands b̅ 2  for Fe 3+  is again several times larger than for the isoelectronic Mn 2+  .

Correlation of Zero Field Splittings and Site Distortions. VII. FeCl 4 - in CsGaCL 4 with Crystal Structure Refinement