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The microwave spectra of CF 3 CN, CH 2 FCN, CHDFCN, CD 2 FCN and CHF 2 CN have been measured and analysed. The nuclear quadrupole hyperfine splittings due to  14 N have been measured by Microwave Fourier Transform spectroscopy. The nuclear quadrupole coupling constants, transformed to the bonding axis systems of the C-C ≡ N groups, are shown to be in accord with structural predictions of the p-electron populations at the nitrogen atom.

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The Rotational Spectra of Fluorinated Acetonitriles;  14 N-nuclear Quadrupole Hyperfine Structures Measured with a Microwave Fourier Transform Spectrometer