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In EPR studies on Fe(III) ions in CdGa 2 S 4  crystals, in accordance with the two different Ga sites two paramagnetic centers could be detected which differ widely in their axial parameter D. An investigation of the crystal field allowed a unique site assignment. A comparison with the Fe(III) resonances in CuGaS 2  and AgGaS 2  does show that the superposition model of Newman and Urban cannot be applied to CdGa 2 S 4  with similar parameters as in the chalcopyrite structures. - A characteristic twinning could be revealed, similar to the “reversed cubic structure” in sphalerite.

Eisenionen als Spinsonden in CdGa 2 S 4 -Kristallen / Fe(III) Ions as Spin Probes in CdGa 2 S 4 Crystals