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The  35 Cl-NQR spectrum of several derivatives of chloral, Cl 3 CCHO, was studied in the ranee 77 K ≦ T ≦ T m . By use of the spin echo double resonance technique a relative assignment of the resonances to different Cl 3 C-groups within one crystallized compound was possible. The solid compounds studied are: High temperature phase of chloral hydrate, Cl 3 CCH(OH) 2 ; parachloral, (Cl 3 CCHO) 3 , (α-and ß-isomer); the two phases of chloral hemihydrate Cl 3 CCHO · 1/2 H 2 O; chloralide (II); chloralhemithiohydrate, Cl 3 CCHO · 1/2 H 2 S. The structure of the molecules in the solid state and the fade out of the NQR resonances are discussed.

Chlorine NQR on Derivatives of Chloral