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The microwave spectra of unstable acetonitrile-N-oxide H 3 1 2 C — 1 2 C — 1 4 N — 1 8 0 and four of its isotopically substituted species have been measured in the frequency range from 7.5 to 32 GHz. The molecule was found to show the spectrum of a symmetric top, thus establishing the linearity of the chain ^ CCNO. From the ground state rotational constants B 0 the fol lowing /^-distances have been evaluated: r ( C C ) = 1 . 4 4 2 A, r ( C N ) = 1 . 1 6 9 A, r ( N O ) = 1 . 2 1 7 A .

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Struktur, Dipolmoment und  14 N-Kernquadrupolkopplungskonstante des Acetonitril-N-Oxids aus dem Mikrowellenspektrum / Structure, Dipole Moment and  14 N-Nuclear Quadrupole Coupling Constant of Acetonitrile-N-Oxide from the Microwave Spectrum