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The hyperfine structure of  99 Tc (IV) in mixed crystals of K 2 [TcCl e ] — K 2  [PtCl 6 ] and K 2  [TcF,] —K 2  [PtF e ] was measured at 3 cm wavelength and at 1.7°K and 77°K respectively. The parameters of the chloro-complex are g max  =1.9896, g min  =1.9876, A max =1.361 × 10 -2  cm -1 , A min  = 1.337 × 10 -2  cm -1 ; in addition to the Δm=0 transitions, the forbidden Δm= ±1 transitions were observed. The parameters of the polycrystalline fluoro-complex were determined to g=3.884, A=3.34 × 10 -2  cm -1 , B=1.76 × 10 -2  cm- 1 .

Paramagnetische Elektronenresonanz von 99 Tc(IV) in Hexahalogeno-Komplexen