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Tm 2 CrB 3 O 9  was obtained by high-pressure/high-temperature syntheses at 7.5 GPa and 850 °C. The compound crystallizes homeotypically to walstromite in the triclinic space groupP1   ¯$P\overline{1}$(no. 2) with the unit cell parameters  a  = 5.9118(4) Å,  b  = 5.9148(4) Å,  c  = 8.3575(6) Å,  α  = 83.64(1)°,  β  = 71.19(1)°, and  γ  = 79.93(1)°, and two formula units per cell. Single-crystal and powder diffraction data are accompanied by an infrared spectroscopic investigation and the structural features of this new compound are discussed in detail.

High-pressure/high-temperature synthesis of the first walstromite-analogue borate Tm 2 CrB 3 O 9