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PrCa 4 O[BO 3 ] 3  was grown as a single crystal by the Czochralski method. The precursor material was synthesized by solid state reaction under O 2  atmosphere and sintered after grinding under N 2  atmosphere with a content of 20% H 2 . The Czochralski crystal growth proceeded under N 2  atmosphere with an &lt;010&gt; oriented GdCa 4 O[BO 3 ] 3  crystal seed. A PrCa 4 O[BO 3 ] 3  crystal with a cylinder length of 20 mm, a diameter of 15 mm, and weight of 23.1 g was obtained. The crystal structure was solved from single crystal X-ray diffraction data in the monoclinic crystal system with space group  C 1 m 1 (No. 8), the lattice parameters  a  = 8.1293(6) Å,  b  = 16.062(1) Å,  c  = 3.6023(2) Å,  β  = 101.371(2)°, formula units of 2 and final  R - and w R 2-values below 3.8%. A mixed occupancy between Pr and Ca of 6.0% was found.

The crystal structure of single crystalline PrCa 4 O[BO 3 ] 3