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Polycrystalline Sc 5 Cu 2 In 4  was synthesized by induction melting of the elements and small single crystals were obtained by a slow cooling sequence. Sc 5 Cu 2 In 4  is the first coinage metal representative in the family of the so-called 5-2-4 intermetallics. The Zr 5 Ir 2 In 4  type structure of Sc 5 Cu 2 In 4  was refined from single crystal X-ray diffractometer data:  Pnma ,  a  = 1716.75(6),  b  = 677.94(12),  c  = 760.69(2) pm,  wR 2 = 0.0531, 1932 F 2  values and 58 variables. Sc 5 Cu 2 In 4  adopts a superstructure of the Lu 5 Ni 2 In 4  type (doubling of the  b  axis and  klassengleiche  symmetry reduction from  Pbam  to  Pnma ), caused by dislocation of the copper atoms (puckering effect). Geometrically, Sc 5 Cu 2 In 4  is a 4:1 intergrowth structure of distorted AlB 2  and CsCl related slabs.

Superstructure formation in Sc 5 Cu 2 In 4