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Beryllium and BeCl 2  were treated with trifluoromethanesulfonic acid and trimethylsilyltriflate, respectively to form beryllium triflates BeL 2 (OTf) 2  (L=H 2 O, THF,   n  Bu 2 O). The Be–O atomic distances (1.605–1.635 Å) between Be 2+  and the triflate anions in solid state are the shortest known distances of this kind in a metal triflate yet. Attempts to remove the solvate molecules led to the decomposition of the obtained compounds.

Beryllium triflates: synthesis and structure of BeL 2 (OTf) 2 (L=H 2 O, THF, n Bu 2 O)