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The molecular and single crystal structure of  O , O -diethyl  O -[2-(dimethylamino)ethyl] phosphorothioate oxalate, as determined by single crystal X-ray diffraction studies, is described for the first time; although this compound is well-known by industry and research from the mid-20 th  century. The known decomposition product of pure  O , O -diethyl  O -[2-(dimethylamino)ethyl] phosphorothioate could also be structurally characterized. Additionally, the compounds are characterized by recent analytical methods e.g. NMR. The findings of our study support the thesis that the isolated decomposition product must be a by-product of the thiono-thiolo rearrangement process of the title compound.

O , O -diethyl O -[2-(dimethylamino)ethyl] phosphorothioate: structural evidence of the decomposition product and its oxalate salt