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The compound RhCd 9+δ  (−1.18≤δ≤0.29) has been synthesized and the average structure has been analyzed by single crystal X-ray diffraction. The average structure crystallizes in the face centered cubic space group  F 4̅3 m  (216) and contains ~405 atoms/unit cell. It represents a (2a γ ) 3 -superstructure of cubic γ-brass and is isostructural to Rh 7−x Mg 44+x . The comparison between the structures of RhCd 9+δ  and Rh 7−x Mg 44+x  has been presented using a layer description. The structure of the title phase has also been described by a “cluster” concept. The electronic structure of RhCd 9+δ  (−1.18≤δ≤0.29) shows that the phase is stabilized by a Hume-Rothery mechanism.

RhCd 9+δ (−1.18≤δ≤0.29) a γ-brass related cubic giant cell structure