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Reaction of benzene-1,2,4,5-tetracarboxylic acid (H 4 L) with Zn(II) salt in DMF/MeOH leads to the formation of the new (μ 2 -benzene-1,2,4,5-tetracarboxylato-O,O′)-hexaaqua-dizinc(II)-dihydrate complex [Zn 2 L(H 2 O) 6 ]·2H 2 O ( 1 ) (L = benzene-1,2,4,5-tetracarboxylate). Crystal structure analysis reveals that each tetracoordinated zinc(II) center adopts a distorted tetrahedral geometry occupied by one O carboxylate  and three O water  atoms. A 3D supramolecular associate in the crystal lattice of  1  has been stabilized by a number of non-covalent interactions (O–H···O). Topology of the H-bonded 3D network has been also analyzed.

Synthesis, supramolecular structure and thermal study of a new dinuclear zinc(II) complex derived from benzene-1,2,4,5-tetracarboxylic acid