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The structural behavior of the non-linear optical, nanoporous compound CsLiB 6 O 10  was studied in a wide temperature range. Both the highly anisotropic thermal expansion of the borate with temperature variation and the deterioration of its crystals were investigated. The electron density distribution was analyzed in detail. A reversible, partial transition to a new modification,  β -CsLiB 6 O 10 , was observed during cooling crystalline and moist samples of CsLiB 6 O 10  to –25 °C. The crystal structure of the new phase is described.

Temperature- and moisture-dependency of CsLiB 6 O 10 . A new phase, β -CsLiB 6 O 10