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In situ  crystallization technique at low temperature was used to obtain single crystals of the low melting compounds N(SiMe 3 ) 3  1  and As(SiMe 3 ) 3  3.  N(SiMe 3 ) 3  has a waxy consistence at room temperature. The solid-state structure of both compounds has been determined by single-crystal X-ray diffraction analysis. N(SiMe 3 ) 3  is distorted and shows nearly a trigonal planar coordination of the central nitrogen atom. In contrast, the heavier homologue As(SiMe 3 ) 3  shows a trigonal pyramidal coordination with Si-As-Si 103.4(6)°–104.9(6)°.

In situ Crystallization of N(SiMe 3 ) 3 and As(SiMe 3 ) 3 : Trigonal planar or pyramidal coordination of the central atoms?