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The molecular complexes of tetrahydrofuran ( THF ) and diethyl ether ( DEE ) with chloroform ( CF ), dichlodromethane ( DCM ) and bromoform ( BF ) have been synthesised by in situ cryo-crystallization and their structures have been determined by single-crystal X-ray diffraction.  CF  forms 2:1 co-crystals with  THF  and  DEE , where the components are linked in isolated 2:1 complexes by Cl 3  C-H…O interactions. Molecules of components in  THF-BF  complex form halogen-bonded chains, while the complexes  DCM  and  BF  with  DEE  contain two independent pairs of the components linked by C-H…O contacts. Supramolecular architecture of the molecular complexes is analysed using energy-based topology of intermolecular interactions.

Low-melting molecular complexes. Part 5. Co-crystals of tetrahydrofuran and diethyl ether with methyl halides