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In this work, a gallium–nickel alloy target with a weight percentage ratio of 7:3 was successfully prepared on Cu substrate in a chloride system at room temperature. A novel organic-solvent-free separation procedure based on two columns for extracting  68 Ge from irradiated Ga–Ni alloy target with high radionuclidic purity (99.99 %) was developed. By this separation procedure, the recovery of  68 Ge is 95 ± 5 % and the yield of  68 Ge via the nuclear reaction  nat Ga(p, x n) 68 Ge was measured to be 0.27 ± 0.02 MBq/μA h.

Efficient extraction of 68 Ge from irradiated Ga–Ni alloy via a novel organic-solvent-free separation procedure