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18 F-fluorination using aluminum-fluoride ([ 18 F]AlF) chelate technique has been reported to give a low-to-moderate radiochemical yield, between 5 and 20%. Therefore, the work described here outlines the optimum  18 F-fluorination condition for the formation of [ 18 F]AlF 2+  and [ 18 F]AlF-NOTA-NHS complex with the radiochemical yield (RCY) and purity (RCP) of more than 90% as a prerequisite step before proceeding with the radiopharmaceutical preparation using the [ 18 F]AlF-bifunctional chelator technique. As well as being simple, the suggested method is practical and relevant for beginners interested in  18 F-fluorination with [ 18 F]AlF-chelate complex technique or also for a researcher who aims to proceed on an extensive scale.

Optimal 18 F-fluorination conditions for the high radiochemical yield of [ 18 F]AlF-NOTA-NHS complexes