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Hollow nanospheres ( ϕ : 60–80 nm, wall thickness: 10–20 nm), consisted of UO 2  nanoparticles ( ϕ : 3–5 nm), were successfully prepared in a Triton X-100-water (50:50, w/w) hexagonal lyotropic liquid crystal (LLC) by γ-irradiation, where water soluble ammonium uranyl tricarbonate was added as precursor. The product was stable at least up to 300°C. Furthermore, whether the nanospheres were hollow or not, and the wall thickness of the hollow nanospheres could be easily controlled  via  adjusting dose rate. While in the Triton X-100 based micellar systems, only solid nanospheres were obtained. At last, a possible combination mechanism containing adsorption, aggregation and fracturing processes was proposed.

Radiolytic syntheses of hollow UO 2 nanospheres in Triton X-100-based lyotropic liquid crystals