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C 52 H 66 N 4 NiO 28 , triclinic,P1   ‾$P\overline{1}$(no. 2),  a  = 11.292(6) Å,  b  = 11.670(6) Å,  c  = 12.165(6) Å,  α  = 81.872(6)°,  β  = 67.036(5)°,  γ  = 75.624(6)°,  V  = 1428.1(12) Å 3 ,  Z  = 1,  R gt  ( F ) = 0.0439,  wR ref  ( F  2 ) = 0.1216, T = 296(2) K.

zeitschrift für kristallographie - new crystal structures

Crystal structure of bis(benzene-1 carboxylato- O  3,5-carboxyl- κ  1 O)-[(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane- κ  4  N,N′,N′′,N′′′ )nickel(II) ─ benzene-1,3,5-tricarboxylic acid ─ water (1/2/4), C 52 H 66 N 4 NiO 28