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C 32 H 18 F 8 O 8 N 2 Rh 2 , monoclinic,  P 2 1 / n  (no. 11),  a  = 9.28200(12) Å,  b  = 11.33638(13) Å,  c  = 16.0352(2) Å,  β  = 105.9326(14)°  V  = 1622.47 Å 3 ,  Z  = 4,  R    gt   ( F ) = 0.0297,  wR    ref   ( F  2 ) = 0.0763, T = 150 K.

The crystal structure of bis(acetonitrile-κ 1 N)tetrakis(μ 2 -2,6-difluorobenzoato-κ 2 O:O′)rhodium(II) (Rh–Rh), C 32 H 18 F 8 O 8 N 2 Rh 2