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C 48 H 32 N 26 Bi 2 , triclinic,  P1   ‾$\overline{1}$(no. 2),  a  = 9.781(5) Å,  b  = 11.667(6) Å,  c  = 11.973(7) Å,  α  = 83.816(10)°,  β  = 74.471(10)°,  γ  = 66.120(8)°,  V  = 1203.7 (11) Å 3 ,  Z  = 1,  R gt  ( F ) = 0.0435, w R ref  ( F  2 ) = 0.1035,  T  = 293 K.

Crystal structure of bis(μ 2 -azido-κ 2 N:N )-tetrakis(azido-κ 1 N )-tetrakis(1,10-phenanthroline-κ 2 N,N ′)dibismuth(III), C 48 H 32 N 26 Bi 2