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C 75 H 76 N 10 O 23 Tb 2 , triclinic,P   −1   ‾$P-\overline{1}$(no. 2),  a  = 10.4524(13) Å,  b  = 12.9626(16) Å,  c  = 15.2003(18) Å,  α  = 108.674(2) ∘ ,  β  = 94.931(2) ∘ ,  γ  = 101.617(2) ∘ ,  V  = 1885.8(4) nm 3 ,  Z  = 1,  Rgt   ( F ) = 0.0236,  wRref   ( F   2 ) = 0.0584, T = 296 K.

zeitschrift für kristallographie - new crystal structures

Solvothermal synthesis and crystal structure of aqua-tris(p-acetamidobenzoate-κ 2 O,O′)-(2,2′-bipyridine-κ 2 N,N′)terbium(III) - water - methanol (1/1/1)