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C 24 H 36 ClN 4 NaNi 2 O 8 , monoclinic,  C 2/ c  (no. 15),  a  = 19.5909(11) Å,  b  = 10.8023(6) Å,  c  = 14.5722(8) Å,  β  = 112.032(1)°,  V  = 2858.7(3) Å 3 ,  Z  = 4,  Rgt   ( F ) = 0.0260,  wRref   ( F   2 ) = 0.0701,  T  = 93(2) K.

Redetermination of the crystal structure of bis[ N , N ′-ethylenebis(acetylacetoniminato)nickel(II)] sodium perchlorate, C 24 H 36 ClN 4 NaNi 2 O 8