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C 26 H 21 Fe 2 O 6 PS 2 , monoclinic,  P 2 1 / c  (no. 14),  a  = 9.0892(6) Å,  b  = 27.6631(18) Å,  c  = 11.3409(8) Å,  β  = 106.409(2)°,  V  = 2735.4(3) Å 3 ,  Z  = 4,  R   gt  ( F ) = 0.0670,  wR   ref  ( F  2 ) = 0.1620, T = 296(2) K.

The crystal structure of pentakis(carbonyl)-{ μ -[2,3-bis(sulfanyl)propan-1-olato]}-(triphenylphosphane)diiron ( Fe – Fe )C 26 H 21 Fe 2 O 6 PS 2